Information card for entry 1570387

Structure parameters

• Common name: PW9
• Formula: C16 H38 Cl P Pd Si
• Calculated formula: C16 H38 Cl P Pd Si
• Title of publication: Visible light-induced palladium-carbon bond weakening in catalytically relevant T-shaped complexes.
• Authors of publication: Waddell, Peter M.; Tian, Lei; Scavuzzo, Anthony R.; Venigalla, Lalu; Scholes, Gregory D.; Carrow, Brad P.
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 48
• Pages of publication: 14217 - 14228
• a: 10.33 ± 0.0004 Å
• b: 15.1751 ± 0.0006 Å
• c: 14.0651 ± 0.0006 Å
• α: 90°
• β: 110.126 ± 0.0018°
• γ: 90°
• Cell volume: 2070.2 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0497
• Weighted residual factors for all reflections included in the refinement: 0.0535
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No