Information card for entry 1570605

Structure parameters

• Formula: C24 H35 B O2 Si
• Calculated formula: C24 H35 B O2 Si
• Title of publication: Borylative transition metal-free couplings of vinyl iodides with various nucleophiles, alkenes or alkynes.
• Authors of publication: Seidler, Gesa; Schwenzer, Max; Clausen, Florian; Daniliuc, Constantin G.; Studer, Armido
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 5
• Pages of publication: 1672 - 1678
• a: 11.8688 ± 0.0002 Å
• b: 17.6865 ± 0.0003 Å
• c: 12.6092 ± 0.0003 Å
• α: 90°
• β: 116.407 ± 0.001°
• γ: 90°
• Cell volume: 2370.71 ± 0.08 ų
• Cell temperature: 101 ± 2 K
• Ambient diffraction temperature: 101 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0586
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.0994
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No