Information card for entry 1570714

Structure parameters

• Formula: C10 H8 Cl4 N8 Si
• Calculated formula: C10 H8 Cl4 N8 Si
• Title of publication: The Hexacoordinate Si Complex SiCl4(4-Azidopyridine)2—Crystallographic Characterization of Two Conformers and Probing the Influence of SiCl4-Complexation on a Click Reaction with Phenylacetylene
• Authors of publication: Riedel, Sophie; Gerwig, Maik; Gerlach, Daniela; Brendler, Erica; Gericke, Robert; Kroke, Edwin; Wagler, Jörg
• Journal of publication: Inorganics
• Year of publication: 2023
• Journal volume: 11
• Journal issue: 12
• Pages of publication: 473
• a: 8.4988 ± 0.0008 Å
• b: 17.5628 ± 0.0015 Å
• c: 11.3833 ± 0.0011 Å
• α: 90°
• β: 101.86 ± 0.007°
• γ: 90°
• Cell volume: 1662.8 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0413
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.0669
• Weighted residual factors for all reflections included in the refinement: 0.0723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No