Information card for entry 1570951

Structure parameters

• Formula: C20 H39 B9 Os2
• Calculated formula: C20 H39 B9 Os2
• Title of publication: Rule breaker boron clusters: a new class of hypoelectronic osmaborane clusters [(Cp*Os)₂B_<i>n</i>H_<i>n</i>] (<i>n</i> = 6-10).
• Authors of publication: Kar, Ketaki; Kar, Sourav; Ghosh, Sundargopal
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 11
• Pages of publication: 4179 - 4186
• a: 8.9252 ± 0.001 Å
• b: 14.6904 ± 0.0016 Å
• c: 20.153 ± 0.002 Å
• α: 90°
• β: 99.649 ± 0.005°
• γ: 90°
• Cell volume: 2605 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0612
• Residual factor for significantly intense reflections: 0.0489
• Weighted residual factors for significantly intense reflections: 0.1139
• Weighted residual factors for all reflections included in the refinement: 0.1278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.133
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No