Information card for entry 1571173

Structure parameters

• Formula: C30 H27 O4 P
• Calculated formula: C30 H27 O4 P
• Title of publication: Pd-catalyzed divergent regioselective annulation of phosphinyl allenes accessing polyarylfurans and 2<i>H</i>-chromenes.
• Authors of publication: Li, Yang; Yan, Xiao-Long; Hu, Li-Yan; Luo, Kai; Zhu, Jie; Wu, Lei
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 28
• Pages of publication: 3814 - 3817
• a: 8.9061 ± 0.0016 Å
• b: 10.4242 ± 0.0018 Å
• c: 14.312 ± 0.003 Å
• α: 74.291 ± 0.005°
• β: 76.463 ± 0.005°
• γ: 86.731 ± 0.005°
• Cell volume: 1243.5 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1135
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for significantly intense reflections: 0.1859
• Weighted residual factors for all reflections included in the refinement: 0.2153
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No