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Information card for entry 1571246
Preview
Coordinates | 1571246.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H26 Cl2 N3 O3 P |
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Calculated formula | C32 H26 Cl2 N3 O3 P |
Title of publication | Cobalt- or rhodium-catalyzed synthesis of 1,2-dihydrophosphete oxides <i>via</i> C-H activation and formal phosphoryl migration. |
Authors of publication | Xu, Shengbo; Mi, Ruijie; Zheng, Guangfan; Li, Xingwei |
Journal of publication | Chemical science |
Year of publication | 2024 |
Journal volume | 15 |
Journal issue | 16 |
Pages of publication | 6012 - 6021 |
a | 9.3078 ± 0.0002 Å |
b | 12.9452 ± 0.0003 Å |
c | 13.3909 ± 0.0003 Å |
α | 83.589 ± 0.001° |
β | 79.897 ± 0.001° |
γ | 69.502 ± 0.001° |
Cell volume | 1485.68 ± 0.06 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0553 |
Residual factor for significantly intense reflections | 0.0459 |
Weighted residual factors for significantly intense reflections | 0.1132 |
Weighted residual factors for all reflections included in the refinement | 0.1222 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1571246.html
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Users of the data should acknowledge the original authors of the
structural data.