Information card for entry 1571317

Structure parameters

• Formula: C55 H139 Fe2 N6 P8 Si4 Sm
• Calculated formula: C55 H139 Fe2 N6 P8 Si4 Sm
• Title of publication: Iron promoted end-on dinitrogen-bridging in heterobimetallic complexes of uranium and lanthanides.
• Authors of publication: Jori, Nadir; Moreno, Juan J.; Shivaraam, R. A. Keerthi; Rajeshkumar, Thayalan; Scopelliti, Rosario; Maron, Laurent; Campos, Jesús; Mazzanti, Marinella
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 18
• Pages of publication: 6842 - 6852
• a: 11.4532 ± 0.0005 Å
• b: 29.5233 ± 0.0009 Å
• c: 23.5755 ± 0.0008 Å
• α: 90°
• β: 97.369 ± 0.004°
• γ: 90°
• Cell volume: 7905.9 ± 0.5 ų
• Cell temperature: 140 ± 0.1 K
• Ambient diffraction temperature: 140 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1143
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.103
• Weighted residual factors for all reflections included in the refinement: 0.1237
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No