Information card for entry 1571321

Structure parameters

• Formula: C38 H102 Fe N5 P4 Si6 Tm
• Calculated formula: C38 H102 Fe N5 P4 Si6 Tm
• Title of publication: Iron promoted end-on dinitrogen-bridging in heterobimetallic complexes of uranium and lanthanides.
• Authors of publication: Jori, Nadir; Moreno, Juan J.; Shivaraam, R. A. Keerthi; Rajeshkumar, Thayalan; Scopelliti, Rosario; Maron, Laurent; Campos, Jesús; Mazzanti, Marinella
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 18
• Pages of publication: 6842 - 6852
• a: 11.6015 ± 0.00016 Å
• b: 18.3958 ± 0.0002 Å
• c: 27.5562 ± 0.0004 Å
• α: 90°
• β: 94.1162 ± 0.0012°
• γ: 90°
• Cell volume: 5865.84 ± 0.13 ų
• Cell temperature: 139.99 ± 0.1 K
• Ambient diffraction temperature: 139.99 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No