Information card for entry 1571343

Structure parameters

• Formula: C52 H77 O10 Si3 Tb
• Calculated formula: C52 H77 O10 Si3 Tb
• Title of publication: Siloxide tripodal ligands as a scaffold for stabilizing lanthanides in the +4 oxidation state.
• Authors of publication: Tricoire, Maxime; Hsueh, Fang-Che; Keener, Megan; Rajeshkumar, Thayalan; Scopelliti, Rosario; Zivkovic, Ivica; Maron, Laurent; Mazzanti, Marinella
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 18
• Pages of publication: 6874 - 6883
• a: 13.9674 ± 0.0004 Å
• b: 18.1707 ± 0.0004 Å
• c: 21.7736 ± 0.0004 Å
• α: 89.0799 ± 0.0015°
• β: 88.765 ± 0.002°
• γ: 87.017 ± 0.002°
• Cell volume: 5516.7 ± 0.2 ų
• Cell temperature: 140.01 ± 0.1 K
• Ambient diffraction temperature: 140.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0585
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No