Crystallography Open Database

Information card for entry 1571354

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Coordinates	1571354.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88.5 H72 K O4 Si4 Tb
Calculated formula	C85 H68 K O4 Si4 Tb
Title of publication	Siloxide tripodal ligands as a scaffold for stabilizing lanthanides in the +4 oxidation state.
Authors of publication	Tricoire, Maxime; Hsueh, Fang-Che; Keener, Megan; Rajeshkumar, Thayalan; Scopelliti, Rosario; Zivkovic, Ivica; Maron, Laurent; Mazzanti, Marinella
Journal of publication	Chemical Science
Year of publication	2024
a	14.0838 ± 0.0014 Å
b	14.2282 ± 0.0017 Å
c	21.775 ± 0.003 Å
α	77.38 ± 0.01°
β	74.179 ± 0.009°
γ	63.234 ± 0.011°
Cell volume	3725 ± 0.9 Å³
Cell temperature	200 ± 0.11 K
Ambient diffraction temperature	200 ± 0.11 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1308
Residual factor for significantly intense reflections	0.085
Weighted residual factors for significantly intense reflections	0.2142
Weighted residual factors for all reflections included in the refinement	0.2509
Goodness-of-fit parameter for all reflections included in the refinement	1.0844
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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