Information card for entry 1571513

Structure parameters

• Common name: 21159z
• Formula: C32 H42 N2 O9 Os Si
• Calculated formula: C32 H42 N2 O9 Os Si
• Title of publication: Cascade reactions of HDDA-benzynes with tethered cyclohexadienones: strain-driven events originating from <i>ortho</i>-annulated benzocyclobutenes.
• Authors of publication: Chinta, Bhavani Shankar; Sneddon, Dorian S.; Hoye, Thomas R.
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 21
• Pages of publication: 8181 - 8189
• a: 12.5341 ± 0.0006 Å
• b: 19.6037 ± 0.0012 Å
• c: 13.2334 ± 0.0006 Å
• α: 90°
• β: 91.919 ± 0.002°
• γ: 90°
• Cell volume: 3249.8 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0477
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0565
• Weighted residual factors for all reflections included in the refinement: 0.0626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No