Crystallography Open Database

Information card for entry 1571538

Preview

Coordinates	1571538.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C119 H108 B2 Cl11 N Os P4
Calculated formula	C119 H108 B2 Cl11 N Os P4
Title of publication	Isomerization reactions of metal vinylidene units.
Authors of publication	Zheng, Xuejuan; Huang, Fanping; Li, Xinyuan; Zhuo, Kaiyue; Chen, Dafa; Luo, Ming; Xia, Haiping
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	22
Pages of publication	8443 - 8450
a	15.7974 ± 0.0005 Å
b	17.7933 ± 0.0005 Å
c	20.4463 ± 0.0006 Å
α	75.963 ± 0.001°
β	89.72 ± 0.001°
γ	73.086 ± 0.001°
Cell volume	5321 ± 0.3 Å³
Cell temperature	100 ± 0.2 K
Ambient diffraction temperature	100 ± 0.2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0516
Residual factor for significantly intense reflections	0.0507
Weighted residual factors for significantly intense reflections	0.1336
Weighted residual factors for all reflections included in the refinement	0.1345
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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