Information card for entry 1571733

Structure parameters

• Formula: C40 H59 Os4 U
• Calculated formula: C40 H59 Os4 U
• Title of publication: Photolysis-driven bond activation by thorium and uranium tetraosmate polyhydride complexes.
• Authors of publication: Ye, Christopher Z.; Del Rosal, Iker; Kelly, Sheridon N.; Brackbill, I. Joseph; Maron, Laurent; Camp, Clément; Arnold, John
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 25
• Pages of publication: 9784 - 9792
• a: 40.875 ± 0.004 Å
• b: 10.0269 ± 0.001 Å
• c: 23.315 ± 0.002 Å
• α: 90°
• β: 113.731 ± 0.004°
• γ: 90°
• Cell volume: 8747.7 ± 1.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0397
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.067
• Weighted residual factors for all reflections included in the refinement: 0.0701
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.7288 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No