Information card for entry 1572025

Structure parameters

• Chemical name: <i>trans</i>-Diaquatetrakis(tetrahydrofuran-κ<i>O</i>)iron(II) μ-carbonyl-tetradecacarbonyltetrachlorido-μ-dimethylsilanediolato-tetragalliumtetrairon(7 <i>Ga</i>–<i>Fe</i>)(<i>Fe</i>–<i>Fe</i>) tetrahydrofuran tetrasolvate
• Formula: C49 H74 Cl4 Fe5 Ga4 O27 Si
• Calculated formula: C49 H74 Cl4 Fe5 Ga4 O27 Si
• Title of publication: trans-Diaquatetrakis(tetrahydrofuran-κO)iron(II) μ-carbonyl-tetradecacarbonyltetrachlorido-μ-dimethylsilanediolato-tetragalliumtetrairon(7 Ga–Fe)(Fe–Fe) tetrahydrofuran tetrasolvate
• Authors of publication: Demmin, Mary Elizabeth; Bauer, Cary; Ruf, Michael; Harakas, George N.
• Journal of publication: IUCrData
• Year of publication: 2024
• Journal volume: 9
• Journal issue: 6
• Pages of publication: x240620
• a: 12.1954 ± 0.0006 Å
• b: 15.2657 ± 0.0007 Å
• c: 39.03 ± 0.0016 Å
• α: 90°
• β: 95.5629 ± 0.0016°
• γ: 90°
• Cell volume: 7232 ± 0.6 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.093
• Weighted residual factors for all reflections included in the refinement: 0.1004
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No