Information card for entry 1572160

Structure parameters

• Formula: C32 H64 N4 S4 U
• Calculated formula: C32 H64 N4 S4 U
• Title of publication: Formation of uranium disulfide from a uranium thioamidate single-source precursor.
• Authors of publication: Kelly, Sheridon N.; Russo, Dominic R.; Ouellette, Erik T.; Roy, Debashree; Swift, Andrew J.; Boreen, Michael A.; Smith, Patrick W.; Moreau, Liane M.; Arnold, John; Minasian, Stefan G.
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 33
• Pages of publication: 13325 - 13332
• a: 21.6654 ± 0.0002 Å
• b: 11.6105 ± 0.0001 Å
• c: 15.6201 ± 0.0001 Å
• α: 90°
• β: 96.284 ± 0.001°
• γ: 90°
• Cell volume: 3905.57 ± 0.06 ų
• Cell temperature: 100 ± 0.11 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0252
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0599
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No