Information card for entry 1572255

Structure parameters

• Chemical name: bis(12-crown-4)lithium tetrakis(trimethylsilylmethyl)vanadate
• Formula: C32 H76 Li O8 Si4 V
• Calculated formula: C32 H76 Li O8 Si4 V
• Title of publication: Coherent spin-control of <i>S</i> = 1 vanadium and molybdenum complexes.
• Authors of publication: Laorenza, Daniel W.; Mullin, Kathleen R.; Weiss, Leah R.; Bayliss, Sam L.; Deb, Pratiti; Awschalom, David D.; Rondinelli, James M.; Freedman, Danna E.
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 34
• Pages of publication: 14016 - 14026
• a: 10.4055 ± 0.0002 Å
• b: 21.3852 ± 0.0003 Å
• c: 20.4877 ± 0.0004 Å
• α: 90°
• β: 104.167 ± 0.002°
• γ: 90°
• Cell volume: 4420.34 ± 0.14 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.0787
• Weighted residual factors for all reflections included in the refinement: 0.0828
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No