Information card for entry 1572521

Structure parameters

• Formula: C22 H66 B14 N2 O32
• Calculated formula: C22 H66 B14 N2 O32
• Title of publication: Tetrahydroxidohexaoxidopentaborate(1-) Salts of C6-Linked Substituted Diimidazolium and Dipyrrolidinium Cations: Synthesis, Characterization and XRD Studies
• Authors of publication: Al-Dulayymi, Ahmad R.; Beckett, Michael A.; Braganca, Radek; Coles, Simon J.; Horton, Peter N.; Rixon, Thomas A.
• Journal of publication: Inorganics
• Year of publication: 2024
• Journal volume: 12
• Journal issue: 8
• Pages of publication: 220
• a: 9.7545 ± 0.0003 Å
• b: 15.4363 ± 0.0004 Å
• c: 17.0325 ± 0.0005 Å
• α: 90°
• β: 101.851 ± 0.003°
• γ: 90°
• Cell volume: 2509.98 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.1443
• Weighted residual factors for all reflections included in the refinement: 0.1483
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No