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Information card for entry 1572802
Preview
Coordinates | 1572802.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H46 B31 O P |
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Calculated formula | C26 H46 B31 O P |
Title of publication | Structure-Constraint Induced Increase in Lewis Acidity of Tris(ortho-carboranyl)borane and Selective Complexation with Bestmann Ylides |
Authors of publication | Xiang, Libo; Wang, Junyi; Matler, Alexander; Ye, Qing |
Journal of publication | Chemical Science |
Year of publication | 2024 |
a | 12.196 ± 0.003 Å |
b | 12.565 ± 0.003 Å |
c | 15.872 ± 0.004 Å |
α | 91.154 ± 0.008° |
β | 106.328 ± 0.009° |
γ | 117.784 ± 0.007° |
Cell volume | 2032.1 ± 0.9 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0562 |
Residual factor for significantly intense reflections | 0.0498 |
Weighted residual factors for significantly intense reflections | 0.1258 |
Weighted residual factors for all reflections included in the refinement | 0.13 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Diffraction radiation X-ray symbol | K-L~2,3~ |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1572802.html
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Users of the data should acknowledge the original authors of the
structural data.