Crystallography Open Database

Information card for entry 1572874

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Coordinates	1572874.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H20 O4
Calculated formula	C24 H20 O4
Title of publication	Three-component modular synthesis of chiral 1,3-dioxoles via Rh-catalyzed carbenic olefination cascade
Authors of publication	Huang, Shisheng; Luo, Jilong; Chen, Ping; Chen, Jiean; Wang, Zhaofeng
Journal of publication	Chemical Science
Year of publication	2024
a	5.57076 ± 0.00008 Å
b	7.79768 ± 0.00012 Å
c	42.0452 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	1826.4 ± 0.05 Å³
Cell temperature	105 ± 2 K
Ambient diffraction temperature	105 ± 2 K
Number of distinct elements	3
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0334
Residual factor for significantly intense reflections	0.0317
Weighted residual factors for significantly intense reflections	0.0792
Weighted residual factors for all reflections included in the refinement	0.0803
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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