Information card for entry 1573004

Structure parameters

• Formula: C24 H27 As4 Mo20 N4 O82 Se2.63
• Calculated formula: C24 H27 As4 Mo20 N4 O82 Se2.63
• Title of publication: Making an inverted Keggin ion lacunary.
• Authors of publication: Liu, Lu-Lu; Xu, Zi-Yu; Yi, Peng; Chen, Chao-Qin; Lang, Zhong-Ling; Yang, Peng
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 41
• Pages of publication: 16977 - 16986
• a: 13.93 ± 0.003 Å
• b: 20.189 ± 0.005 Å
• c: 24.369 ± 0.006 Å
• α: 91.991 ± 0.007°
• β: 99.609 ± 0.008°
• γ: 90.075 ± 0.008°
• Cell volume: 6753 ± 3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1878
• Residual factor for significantly intense reflections: 0.141
• Weighted residual factors for significantly intense reflections: 0.3559
• Weighted residual factors for all reflections included in the refinement: 0.3731
• Goodness-of-fit parameter for all reflections included in the refinement: 1.226
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No