Information card for entry 1573760

Structure parameters

• Formula: C24 H25 I N2 O
• Calculated formula: C24 H25 I N2 O
• Title of publication: Stereoselective synthesis of atropisomeric amides enabled by intramolecular acyl transfer.
• Authors of publication: Wootton, Jack M.; Roper, Natalie J.; Morris, Catrin E.; Maguire, Victoria E.; Duff, Lee C.; Waddell, Paul G.; Whitwood, Adrian C.; Gammons, Richard J.; Miah, Afjal H.; Lynam, Jason M.; Armstrong, Roly J.; Unsworth, William P.
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 9
• Pages of publication: 3938 - 3945
• a: 8.6576 ± 0.0003 Å
• b: 11.4823 ± 0.0004 Å
• c: 11.8769 ± 0.0005 Å
• α: 70.882 ± 0.004°
• β: 79.329 ± 0.003°
• γ: 82.137 ± 0.003°
• Cell volume: 1092.57 ± 0.08 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0853
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No