Information card for entry 1574358

Structure parameters

• Formula: C56 H102 As8 K N2 O9 Ta2
• Calculated formula: C48 H86 As8 K N2 O7 Ta2
• Title of publication: Redox mediated dimerisation of a cyclo-As8 complex
• Authors of publication: Riesinger, Christoph; Scheer, Manfred
• Journal of publication: Chemical Science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 20
• Pages of publication: 8807 - 8811
• a: 15.0711 ± 0.0003 Å
• b: 15.7076 ± 0.0002 Å
• c: 17.5064 ± 0.0004 Å
• α: 109.325 ± 0.002°
• β: 108.365 ± 0.002°
• γ: 101.944 ± 0.001°
• Cell volume: 3480.31 ± 0.15 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0569
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.1494
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No