Crystallography Open Database

Information card for entry 1574960

Preview

Coordinates	1574960.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H79 Al N5 P Si
Calculated formula	C46 H79 Al N5 P Si
Title of publication	Aluminacyclopropene-phosphine complex: a carbene-exchange reagent.
Authors of publication	Xu, Huihui; León Baeza, José Miguel; Baceiredo, Antoine; Rojas Guerrero, René Segundo; Saffon-Merceron, Nathalie; Branchadell, Vicenç; Kato, Tsuyoshi
Journal of publication	Chemical science
Year of publication	2025
Journal volume	16
Journal issue	31
Pages of publication	14225 - 14230
a	13.896 ± 0.0014 Å
b	17.3957 ± 0.0016 Å
c	19.5978 ± 0.0017 Å
α	90°
β	104.351 ± 0.003°
γ	90°
Cell volume	4589.6 ± 0.7 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.23
Residual factor for significantly intense reflections	0.1028
Weighted residual factors for significantly intense reflections	0.2089
Weighted residual factors for all reflections included in the refinement	0.2851
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1574960.html