Information card for entry 2000016

Structure parameters

• Formula: C32 H72 Cl14 N2 W6
• Calculated formula: C56 H126 Cl28 N2 W12
• Title of publication: An Improved High Yield Synthesis Procedure and Reactivity of W~6~S~8~(4-tert-butylpyridine)~6~
• Authors of publication: Venkataraman, D.; Rayburn, Lori L.; Hill, Laurie I.; Jin, Song; Malik, Abds-Sami; Turneau, Kevin J.; DiSalvo, Francis J.
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 828 - 830
• a: 12.825 ± 0.002 Å
• b: 11.691 ± 0.002 Å
• c: 18.568 ± 0.005 Å
• α: 90°
• β: 90.15 ± 0.03°
• γ: 90°
• Cell volume: 2784.02 ų
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.0496
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No