Information card for entry 2000497

Structure parameters

• Formula: C12 H28 P2 S4
• Calculated formula: C12 H28 P2 S4
• Title of publication: Structures of bis(dialkylthiophosphoryl) disulfides, [<i>R</i>~2~P(S)]~2~S~2~, <i>R</i> = Me, ^<i>i^</i>Pr, and the question of P-S π bonding
• Authors of publication: Gallacher, A. C.; Pinkerton, A. A.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1992
• Journal volume: 48
• Journal issue: 11
• Pages of publication: 2085 - 2088
• a: 7.616 ± 0.001 Å
• b: 11.378 ± 0.001 Å
• c: 12.403 ± 0.002 Å
• α: 68.33 ± 0.01°
• β: 72.61 ± 0.01°
• γ: 85.53 ± 0.01°
• Cell volume: 952.5 ± 0.2 ų
• Cell temperature: 294 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for significantly intense reflections: 0.032
• Goodness-of-fit parameter for significantly intense reflections: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No