Information card for entry 2001160

Structure parameters

• Formula: C12 H31 Cl2 N5 Ni O8
• Calculated formula: C12 H31 Cl2 N5 Ni O8
• Title of publication: Structure of (2,5,9,13,16-pentaazaheptadecane)perchloratonickel(II) perchlorate, [Ni(ClO~4~)(C~12~H~31~N~5~)](ClO~4~)
• Authors of publication: Tahirov, T. H.; Lu, T.-H.; Liu, Y.-L.; Huang, C.-C.; Yuan, Y.-Z.; Chung, C.-S.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1993
• Journal volume: 49
• Journal issue: 12
• Pages of publication: 2114 - 2115
• a: 9.889 ± 0.003 Å
• b: 25.239 ± 0.004 Å
• c: 8.402 ± 0.002 Å
• α: 90°
• β: 92.85 ± 0.02°
• γ: 90°
• Cell volume: 2094.4 ± 0.9 ų
• Cell temperature: 298 ± 3 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.069
• Weighted residual factors for significantly intense reflections: 0.08
• Goodness-of-fit parameter for significantly intense reflections: 24.27
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No