Information card for entry 2001523

Structure parameters

• Formula: C32 H33 N2 Ni P3 S2
• Calculated formula: C32 H33 N2 Ni P3 S2
• Title of publication: Structures of nickel(II) bis- and trisphosphine diisothiocyanate complexes
• Authors of publication: Juma, B.; Fronczek, F. R.; Stanley, G. G.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1993
• Journal volume: 49
• Journal issue: 7
• Pages of publication: 1325 - 1328
• a: 7.602 ± 0.002 Å
• b: 20.599 ± 0.002 Å
• c: 20.712 ± 0.004 Å
• α: 90°
• β: 97.98 ± 0.02°
• γ: 90°
• Cell volume: 3212 ± 1.1 ų
• Cell temperature: 298 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.081
• Weighted residual factors for significantly intense reflections: 0.089
• Goodness-of-fit parameter for significantly intense reflections: 3.23
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No