Information card for entry 2001707

Structure parameters

• Formula: C10 H25 Cl2 N5 Ni O8
• Calculated formula: C10 H25 Cl2 N5 Ni O9
• Title of publication: Structure of (1,4,7,10,13-Pentaazacyclopentadecane-<i>N</i>^1^,<i>N</i>^4^,<i>N</i>^10^,<i>N</i>^13^)(perchlorato-<i>O</i>)nickel(II) perchlorate
• Authors of publication: Lu, T.-H.; Lan, W.-J.; Chung, C.-S.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1993
• Journal volume: 49
• Journal issue: 5
• Pages of publication: 961 - 963
• a: 9.822 ± 0.005 Å
• b: 13.676 ± 0.007 Å
• c: 13.998 ± 0.004 Å
• α: 90°
• β: 96.86 ± 0.03°
• γ: 90°
• Cell volume: 1866.8 ± 1.5 ų
• Cell temperature: 298 ± 3 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.066
• Weighted residual factors for significantly intense reflections: 0.074
• Goodness-of-fit parameter for significantly intense reflections: 2.03
• Diffraction radiation wavelength: 0.7093 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No