Information card for entry 2003321

Structure parameters

• Chemical name: azidotetrakis(trimethylphosphine)nickel(II) tetrafluoroborate
• Formula: C12 H36 B F4 N3 Ni P4
• Calculated formula: C12 H36 B F4 N3 Ni P4
• Title of publication: Azidotetrakis(trimethylphosphine)nickel(II) Tetrafluoroborate
• Authors of publication: Carson, C. C.; Pike, R. D.; Carpenter, G. B.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 4
• Pages of publication: 595 - 598
• a: 13.778 ± 0.002 Å
• b: 13.2816 ± 0.0013 Å
• c: 26.188 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4792.2 ± 1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1242
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections: 0.1529
• Weighted residual factors for significantly intense reflections: 0.1337
• Goodness-of-fit parameter for all reflections: 0.852
• Goodness-of-fit parameter for significantly intense reflections: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No