Information card for entry 2003371

Structure parameters

• Formula: C14 H30 B10 Si
• Calculated formula: C14 H30 B10 Si
• Title of publication: Steric Effects in Heteroboranes. VI. 1-Ph-2-^<i>t^</i>BuMe~2~Si-1,2-<i>closo</i>-C~2~B~10~H~10~
• Authors of publication: McGrath, T. D.; Welch, A. J.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 4
• Pages of publication: 654 - 657
• a: 9.3854 ± 0.0019 Å
• b: 10.2938 ± 0.0026 Å
• c: 13.061 ± 0.005 Å
• α: 68.607 ± 0.025°
• β: 70.281 ± 0.024°
• γ: 64.998 ± 0.017°
• Cell volume: 1039.4 ± 0.6 ų
• Cell temperature: 293 ± 1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.0939
• Goodness-of-fit parameter for significantly intense reflections: 1.351
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No