Information card for entry 2003585

Structure parameters

• Formula: C34 H39 N O3 Si
• Calculated formula: C34 H39 N O3 Si
• Title of publication: (1<i>R</i>*,3<i>S</i>*,4<i>R</i>*)-4-<i>tert</i>-Butyldiphenylsilyloxy-6,7-dimethoxy-1-methyl-3-phenyl-1,2,3,4-tetrahydroisoquinoline
• Authors of publication: Urtiaga, M. K.; Arriortua, M. I.; Tellitu, I.; Badía, D.; Domínguez, E.; Ochando, L.; Amigó, J. M.; Debaerdemaeker, T.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 6
• Pages of publication: 1232 - 1234
• a: 13.747 ± 0.009 Å
• b: 21.08 ± 0.04 Å
• c: 10.3 ± 0.01 Å
• α: 90°
• β: 98.97 ± 0.06°
• γ: 90°
• Cell volume: 2948 ± 7 ų
• Cell temperature: 295 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.071
• Weighted residual factors for significantly intense reflections: 0.094
• Goodness-of-fit parameter for significantly intense reflections: 1.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No