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Information card for entry 2003730
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Coordinates | 2003730.cif |
---|---|
Original IUCr paper | HTML |
Chemical name | [C,O-(2-acetylbicyclohept[2.2.1]-3-yl)palladium(II)(2,2'-bipyridyl)] trifluoromethanesulfonate 0.5 diethylether solvate |
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Formula | C44 H52 F6 N4 O9 Pd2 S2 |
Calculated formula | C22 H26 F3 N2 O4.5 Pd S |
Title of publication | (2-Acetylbicyclo[2.2.1]heptyl-<i>C</i>^3^,<i>O</i>)(2,2'-bipyridyl)palladium(II) Trifluoromethanesulfonate 0.5-Diethyl Ether Solvate |
Authors of publication | Spek, A. L.; Markies, B. A.; Kruis, D.; Boersma, J.; van Koten, G. |
Journal of publication | Acta Crystallographica Section C |
Year of publication | 1995 |
Journal volume | 51 |
Journal issue | 8 |
Pages of publication | 1535 - 1537 |
a | 14.3658 ± 0.0012 Å |
b | 11.0537 ± 0.0006 Å |
c | 19.3767 ± 0.0007 Å |
α | 90° |
β | 128.707 ± 0.005° |
γ | 90° |
Cell volume | 2401.1 ± 0.3 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for significantly intense reflections | 0.037 |
Weighted residual factors for significantly intense reflections | 0.043 |
Goodness-of-fit parameter for significantly intense reflections | 1.4 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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