Information card for entry 2003741

Structure parameters

• Chemical name: closo-[(3-tert-Butylisocyanide)-3,8-bis(dimethylphenylphosphine)- octahydro-1,2-diarsenanonaborato(1-)-3-palladium(II)(1+)] Hexafluoroantimonate
• Formula: C21 H39 As2 B9 F6 N P2 Pd Sb
• Calculated formula: C21 H39 As2 B9 F6 N P2 Pd Sb
• Title of publication: (3-<i>tert</i>-Butyl isocyanide)-3,8-bis(dimethylphenylphosphine)octahydro-1,2-diarsa-3-pallada-<i>closo</i>-dodecaboron(1+) Hexafluoroantimonate
• Authors of publication: Ferguson, G.; Li, Y.; Spalding, T. R.; Patterson, J. C.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 8
• Pages of publication: 1498 - 1500
• a: 9.9342 ± 0.0008 Å
• b: 13.0495 ± 0.0013 Å
• c: 15.3141 ± 0.0014 Å
• α: 96.612 ± 0.0009°
• β: 102.291 ± 0.001°
• γ: 105.039 ± 0.008°
• Cell volume: 1842.5 ± 0.3 ų
• Cell temperature: 291 ± 1 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0899
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for all reflections: 0.1176
• Weighted residual factors for significantly intense reflections: 0.1071
• Goodness-of-fit parameter for all reflections: 1.026
• Goodness-of-fit parameter for significantly intense reflections: 1.216
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No