Information card for entry 2003866

Structure parameters

• Formula: C36 H20 O8 Ru3
• Calculated formula: C36 H20 O8 Ru3
• Title of publication: Alkyne Coupling Induced by a Trinuclear Ruthenium Cluster: Synthesis and Structure of Di-μ-carbonyl-hexacarbonyl-μ~3~-(1,2,3,4-tetraphenyl-1,3-butadiene-1,4-diyl)-triruthenium(2 <i>Ru</i>—<i>Ru</i>), [Ru~3~(CO)~8~(C~4~Ph~4~)]
• Authors of publication: Capparelli, M. V.; De Sanctis, Y.; Arce, A. J.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 9
• Pages of publication: 1819 - 1822
• a: 9.556 ± 0.003 Å
• b: 18.694 ± 0.004 Å
• c: 18.465 ± 0.002 Å
• α: 90°
• β: 95.77 ± 0.01°
• γ: 90°
• Cell volume: 3281.9 ± 1.3 ų
• Cell temperature: 295 ± 1 K
• Ambient diffraction temperature: 295 ± 5 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.049
• Goodness-of-fit parameter for significantly intense reflections: 2.012
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No