Information card for entry 2003936

Structure parameters

• Chemical name: (Z)-N-[(2R,3R)-2-(tert-Butoxycarbonylamino)-3-(tert- butyldiphenylsilyloxy)butylidene]benzylamine N-oxide
• Formula: C32 H42 N2 O4 Si
• Calculated formula: C32 H42 N2 O4 Si
• SMILES: [Si](O[C@@H]([C@H](NC(=O)OC(C)(C)C)C=N(=O)Cc1ccccc1)C)(C(C)(C)C)(c1ccccc1)c1ccccc1
• Title of publication: (<i>Z</i>)-<i>N</i>-[(2<i>R</i>,3<i>R</i>)-2-(<i>tert</i>-Butoxycarbonylamino)-3-(<i>tert</i>-butyldiphenylsiloxy)butylidene]benzylamine <i>N</i>-Oxide
• Authors of publication: Merino, P.; Merchan, F. L.; Tejero, T.; Lanaspa, A.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 9
• Pages of publication: 1949 - 1950
• a: 10.002 ± 0.002 Å
• b: 14.274 ± 0.003 Å
• c: 21.976 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3137.5 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1279
• Residual factor for significantly intense reflections: 0.0568
• Weighted residual factors for all reflections: 0.1593
• Weighted residual factors for significantly intense reflections: 0.1148
• Goodness-of-fit parameter for all reflections: 1.078
• Goodness-of-fit parameter for significantly intense reflections: 1.132
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No