Information card for entry 2005063

Structure parameters

• Chemical name: μ-Chloro-bis-{([9R^*^,12R^*^]-6,8,8,13,13,15-hexamethyl-1,5,9,12- tetraazacyclopentadeca-5,15(1)-diene-N^1^,N^5^,N^9^,N^12^)- perchlorato)copper(II)} perchlorate
• Formula: C17 H34 Cl2 Cu N4 O6
• Calculated formula: C17 H31 Cl2 Cu N4 O6
• Title of publication: A Chloro-Bridged Dinuclear Copper(II) Cationic Complex of a 15-Membered Tetraaza Macrocyclic Ligand
• Authors of publication: Gladkikh, O. P.; Curtis, N. F.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1996
• Journal volume: 52
• Journal issue: 6
• Pages of publication: 1418 - 1421
• a: 11.379 ± 0.003 Å
• b: 12.708 ± 0.002 Å
• c: 16.241 ± 0.003 Å
• α: 90°
• β: 100.11 ± 0.02°
• γ: 90°
• Cell volume: 2312.1 ± 0.8 ų
• Cell temperature: 141 ± 2 K
• Ambient diffraction temperature: 141 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0953
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for all reflections: 0.1567
• Weighted residual factors for significantly intense reflections: 0.1387
• Goodness-of-fit parameter for all reflections: 1.009
• Goodness-of-fit parameter for significantly intense reflections: 1.145
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No