Information card for entry 2005310

Structure parameters

• Formula: C36 H46 N4 O12 V4
• Calculated formula: C36 H46 N4 O12 V4
• Title of publication: A Mixed-Valence Tetranuclear Vanadium(IV, V) Complex, [V~4~O~4~(μ-OEt)~2~(μ-O)~2~(OEt)~4~(phen)~2~]
• Authors of publication: Kumagai, H.; Endo, M.; Kawata, S.; Kitagawa, S.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1996
• Journal volume: 52
• Journal issue: 8
• Pages of publication: 1943 - 1945
• a: 8.971 ± 0.001 Å
• b: 15.511 ± 0.002 Å
• c: 8.329 ± 0.001 Å
• α: 102.85 ± 0.01°
• β: 111.46 ± 0.01°
• γ: 73.67 ± 0.01°
• Cell volume: 1025.8 ± 0.2 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for significantly intense reflections: 0.054
• Goodness-of-fit parameter for significantly intense reflections: 3.53
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No