Information card for entry 2005359

Structure parameters

• Chemical name: Chlorobis[1,2-bis-(diphenylphosphino)ethane]osmium(II) Hexafluorophosphate Dichoromethane Solvate
• Formula: C53.5 H51 Cl4 F6 Os P5
• Calculated formula: C53.5 H51 Cl4 F6 Os P5
• Title of publication: Bis[1,2-bis(diphenylphosphino)ethane-<i>P</i>,<i>P</i>']chloroosmium(II) Hexafluorophosphate Dichloromethane Solvate
• Authors of publication: Lough, A. J.; Morris, R. H.; Schlaf, M.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1996
• Journal volume: 52
• Journal issue: 9
• Pages of publication: 2193 - 2196
• a: 12.298 ± 0.001 Å
• b: 15.685 ± 0.002 Å
• c: 27.851 ± 0.004 Å
• α: 90°
• β: 100.51 ± 0.01°
• γ: 90°
• Cell volume: 5282.2 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for all reflections: 0.0797
• Weighted residual factors for significantly intense reflections: 0.0697
• Goodness-of-fit parameter for all reflections: 1.042
• Goodness-of-fit parameter for significantly intense reflections: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No