Information card for entry 2005758

Structure parameters

• Chemical name: β-meso (5,7,7,12,12,14-hexamethyl-1,4,8,11-tetraazzcyclo- tetradecane) Nickel(II) Diperchlorate Monohydrate
• Formula: C16 H38 Cl2 N4 Ni O9
• Calculated formula: C16 H38 Cl2 N4 Ni O9
• Title of publication: β-<i>meso</i>-(5,7,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) Diperchlorate Monohydrate
• Authors of publication: Wang, A.; Lee, T.-J.; Chen, B.-H.; Yuan, Y.-Z.; Chung, C.-S.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1996
• Journal volume: 52
• Journal issue: 12
• Pages of publication: 3033 - 3035
• a: 17.494 ± 0.003 Å
• b: 9.172 ± 0.002 Å
• c: 17.388 ± 0.003 Å
• α: 90°
• β: 116.7 ± 0.1°
• γ: 90°
• Cell volume: 2492 ± 2 ų
• Cell temperature: 298 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0596
• Weighted residual factors for significantly intense reflections: 0.0581
• Goodness-of-fit parameter for significantly intense reflections: 1.81
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No