Information card for entry 2006656

Structure parameters

• Chemical name: bis(acetonitrile)tetrakis(N,N-dimethylacetamide)nickel(II) tetrafluoroborate
• Formula: C20 H42 B2 F8 N6 Ni O4
• Calculated formula: C20 H42 B2 F8 N6 Ni O4
• Title of publication: Steric Hindrance in a Mixed Solvated Nickel(II) Complex: Bis(acetonitrile-<i>N</i>)tetrakis(<i>N</i>,<i>N</i>-dimethylacetamide-<i>O</i>)nickel(II) Bis(tetrafluoroborate)
• Authors of publication: Suzuki, Honoh; Ishiguro, Shin-ichi
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1997
• Journal volume: 53
• Journal issue: 11
• Pages of publication: 1602 - 1605
• a: 6.892 ± 0.003 Å
• b: 19.706 ± 0.005 Å
• c: 11.842 ± 0.002 Å
• α: 90°
• β: 94.24 ± 0.02°
• γ: 90°
• Cell volume: 1603.9 ± 0.9 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0984
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for all reflections: 0.1825
• Weighted residual factors for significantly intense reflections: 0.1453
• Goodness-of-fit parameter for all reflections: 1.152
• Goodness-of-fit parameter for significantly intense reflections: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No