Information card for entry 2007087

Structure parameters

• Formula: C15 H32 I6 N6 Ni
• Calculated formula: C15 H32 I6 N6 Ni
• Title of publication: Bis(acetonitrile-<i>N</i>)(1,4,8,12-tetraazacyclopentadecane)nickel(II) Bis(triiodide) and (1,4,8,12-Tetraazacyclopentadecane)palladium(II) Bis(triiodide)
• Authors of publication: Blake, Alexander J.; Li, Wan-Sheung; Lippolis, Vito; Schröder, Martin
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1998
• Journal volume: 54
• Journal issue: 3
• Pages of publication: 299 - 302
• a: 16.885 ± 0.006 Å
• b: 18.689 ± 0.004 Å
• c: 9.452 ± 0.003 Å
• α: 90°
• β: 94.05 ± 0.05°
• γ: 90°
• Cell volume: 2975.3 ± 1.6 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for all reflections included in the refinement: 0.0948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No