Information card for entry 2007556

Structure parameters

• Formula: C22 H35 N3 Si2 W
• Calculated formula: C22 H35 N3 Si2 W
• Title of publication: [<i>N</i>,<i>N</i>'-Bis(trimethylsilyl)-<i>o</i>-phenylenediamido](1,4-butanediyl)(phenylimido)tungsten(VI), a Deactivation Product from Olefin Metathesis Polymerization
• Authors of publication: Wang, Shu-Yu S.; Boncella, James M.; Abboud, Khalil A.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1998
• Journal volume: 54
• Journal issue: 8
• Pages of publication: IUC9800035
• a: 9.2118 ± 0.0001 Å
• b: 12.0569 ± 0.0002 Å
• c: 12.0845 ± 0.0002 Å
• α: 104.471 ± 0.001°
• β: 97.954 ± 0.001°
• γ: 102.247 ± 0.001°
• Cell volume: 1243.77 ± 0.03 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0293
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0564
• Weighted residual factors for all reflections included in the refinement: 0.0588
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No