Information card for entry 2007660

Structure parameters

• Chemical name: Bis[μ-methylenebis(dicyclohexylphosphine)- P:P']bis[chloropalladium(I)](Pd—Pd) Bis(acetonitrile) Solvate
• Formula: C54 H98 Cl2 N2 P4 Pd2
• Calculated formula: C54 H98 Cl2 N2 P4 Pd2
• Title of publication: Bis[μ-methylenebis(dicyclohexylphosphine)-<i>P</i>:<i>P</i>']bis[chloropalladium(I)](<i>Pd</i>—<i>Pd</i>) Diacetonitrile Solvate
• Authors of publication: Hashioka, Miho; Sakai, Ken; Tsubomura, Taro
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1998
• Journal volume: 54
• Journal issue: 9
• Pages of publication: 1244 - 1247
• a: 28.021 ± 0.005 Å
• b: 17.118 ± 0.004 Å
• c: 12.11 ± 0.002 Å
• α: 90°
• β: 90.44 ± 0.02°
• γ: 90°
• Cell volume: 5809 ± 2 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.16
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for all reflections: 0.184
• Weighted residual factors for significantly intense reflections: 0.121
• Goodness-of-fit parameter for all reflections: 1.034
• Goodness-of-fit parameter for significantly intense reflections: 1.069
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes