Information card for entry 2008202

Structure parameters

• Chemical name: (μ~2~-Hydrydo)-(μ~2~-N-methylcarboxamido-C,O)-trimethylamine)- nonacarbonyl- tri-osmium
• Formula: C14 H14 N2 O10 Os3
• Calculated formula: C14 H14 N2 O10 Os3
• SMILES: [Os]12([Os]3([Os]2([H]3)(C(O1)NC)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])([N](C)(C)C)(C#[O])C#[O]
• Title of publication: Nonacarbonyl-μ~2~-hydrido-μ~2~-(<i>N</i>-methylcarboxamido)-<i>C</i>:<i>O</i>-(<i>N</i>-trimethylamine)triosmium(3 <i>Os</i>—<i>Os</i>)
• Authors of publication: Andrés Vega; Evgenia Spodine; Alejandro Arce; Jorge Manzur; Ana María García; María Teresa Garland
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 3
• Pages of publication: 322 - 323
• a: 12.932 ± 0.002 Å
• b: 11.273 ± 0.002 Å
• c: 14.921 ± 0.003 Å
• α: 90°
• β: 100.16 ± 0.014°
• γ: 90°
• Cell volume: 2141.1 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0659
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for all reflections: 0.0787
• Weighted residual factors for significantly intense reflections: 0.0671
• Goodness-of-fit parameter for all reflections: 1.016
• Goodness-of-fit parameter for significantly intense reflections: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No