Information card for entry 2009253

Structure parameters

• Chemical name: bis[(μ~3~-oxo)-μ~2~-(2-formylbenzoato-O,O')-(2-formylbenzoato-O)-bis(dibutyl- tin(IV)]
• Formula: C64 H92 O14 Sn4
• Calculated formula: C64 H92 O14 Sn4
• Title of publication: 3-Hydroxyphthalide and its adduct with dibutyltin oxide
• Authors of publication: Khoo, Lian Ee; Hazell, Alan
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 12
• Pages of publication: 2070 - 2073
• a: 12.1605 ± 0.0006 Å
• b: 12.414 ± 0.0006 Å
• c: 25.061 ± 0.001 Å
• α: 83.771 ± 0.001°
• β: 82.672 ± 0.001°
• γ: 62.875 ± 0.001°
• Cell volume: 3334.2 ± 0.3 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for all reflections included in the refinement: 0.037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.243
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No