Information card for entry 2009310

Structure parameters

• Chemical name: Diaqua{hydrogen bis[1-(pyridin-2-yl)ethanone oximato-N,N']}nickel(II) perchlorate hydrate.
• Formula: C14 H21 Cl N4 Ni O9
• Calculated formula: C14 H21 Cl N4 Ni O9
• Title of publication: Diaqua{hydrogen bis[1-(2-pyridyl)ethanone oximato-<i>N</i>,<i>N</i>']}nickel(II) perchlorate hydrate
• Authors of publication: Pajunen, Aarne; Orama, Marjatta; Saarinen, Heikki
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 12
• Pages of publication: 2075 - 2077
• a: 10.586 ± 0.002 Å
• b: 11.925 ± 0.002 Å
• c: 7.803 ± 0.002 Å
• α: 90°
• β: 105.64 ± 0.03°
• γ: 90°
• Cell volume: 948.6 ± 0.4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.03
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No