Information card for entry 2009466

Structure parameters

• Formula: C34 H33 N3 O P Pd
• Calculated formula: C34 H33 N3 O P Pd
• Title of publication: Hybrid ligands. Structure of a palladium(II) complex containing a pyrazolol-derived phosphine ligand, [(<i>o</i>-C~6~H~4~CH~2~NMe~2~)Pd(Ph~2~P{ṟidge{Cḅ C(O)N(Ph)Nḅ C}{33mm}(Me)})]
• Authors of publication: Matt, D.; Guillemin, J.-C.; Ziessel, R.; Balegroune, F.; Grandjean, D.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1994
• Journal volume: 50
• Journal issue: 2
• Pages of publication: 193 - 195
• a: 12.148 ± 0.012 Å
• b: 18.36 ± 0.007 Å
• c: 14.815 ± 0.004 Å
• α: 90°
• β: 112.39 ± 0.04°
• γ: 90°
• Cell volume: 3055 ± 3 ų
• Cell temperature: 294 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.053
• Goodness-of-fit parameter for significantly intense reflections: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No