Information card for entry 2010247

Structure parameters

• Formula: C42 H56 F24 N8 O8 P4 Re2
• Calculated formula: C42 H56 F24 N8 O8 P4 Re2
• Title of publication: Di-μ-oxo-bis{[tris(2-pyridylmethyl)amine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''']rhenium(IV)} tetrakis(hexafluorophosphate) diacetone tetrahydrate
• Authors of publication: Takahira, T.; Umakoshi, K.; Sasaki, Y.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1994
• Journal volume: 50
• Journal issue: 12
• Pages of publication: 1870 - 1872
• a: 13.192 ± 0.004 Å
• b: 13.865 ± 0.006 Å
• c: 9.822 ± 0.003 Å
• α: 104.02 ± 0.03°
• β: 110.14 ± 0.02°
• γ: 106.22 ± 0.03°
• Cell volume: 1501.1 ± 1.1 ų
• Cell temperature: 296 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.051
• Goodness-of-fit parameter for significantly intense reflections: 1.73
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No