Information card for entry 2010529

Structure parameters

• Chemical name: trans-[hydrotetrakis(trimethylphosphine)Rhodiumchloride/bromide] [(tetrabromobenzene-1,2-diolato)borate] dichloromethane solvate
• Formula: C25 H39 B Br8.27 Cl2.73 O4 P4 Rh
• Calculated formula: C25 H39 B Br8.26 Cl2.74 O4 P4 Rh
• Title of publication: Compositional disorder in <i>trans</i>-[RhBr~0.26~Cl~0.74~H(PMe~3~)~4~][B(1,2-O~2~C~6~Br~4~)]·CH~2~Cl~2~
• Authors of publication: Norman, Nicholas C.; Orpen, A. Guy; Quayle, Michael J.; Robins, Edward G.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2000
• Journal volume: 56
• Journal issue: 1
• Pages of publication: 50 - 52
• a: 13.014 ± 0.0009 Å
• b: 16.399 ± 0.0015 Å
• c: 20.726 ± 0.003 Å
• α: 90 ± 0.008°
• β: 90 ± 0.01°
• γ: 90 ± 0.009°
• Cell volume: 4423.3 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0703
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for all reflections: 0.1184
• Weighted residual factors for all reflections included in the refinement: 0.1126
• Goodness-of-fit parameter for all reflections: 1.031
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes