Information card for entry 2010668

Structure parameters

• Chemical name: Dimethyl[1,3-bis(diphenylphosphino)propane]palladium(II) hemitoluene
• Formula: C32.5 H36 P2 Pd
• Calculated formula: C32.5 H36 P2 Pd
• Title of publication: An alkyl‒palladium(II) complex with a bidentate phosphine ligand: [1,3-bis(diphenylphosphino)propane-<i>P</i>,<i>P</i>']dimethylpalladium(II) toluene hemisolvate
• Authors of publication: Abu-Surrah, Adnan S.; Debaerdemaeker, Tony; Huhn, Wolfgang; Rieger, Bernhard; Klinga, Martti; Repo, Timo; Leskelä, Markku
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2000
• Journal volume: 56
• Journal issue: 2
• Pages of publication: e42 - e43
• a: 12.26 ± 0.003 Å
• b: 15.025 ± 0.002 Å
• c: 16.347 ± 0.003 Å
• α: 90°
• β: 99 ± 0.02°
• γ: 90°
• Cell volume: 2974.2 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.03
• Residual factor for significantly intense reflections: 0.023
• Weighted residual factors for all reflections included in the refinement: 0.062
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes